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Materials SciencesCrystallography

Laboratory for X-Ray Optics

Authors: Charles M. Falco; ARIZONA UNIV TUCSON OPTICAL SCIENCES CENTER
Abstract:
During this period we concentrated our effort in two areas: (1) growth of epitaxial single-crystal beryllium films; and (2) multilayers and interfaces of material pairs incorporating 'new' materials for multilayer x-ray optics. To date we have succeeded in growing epitaxial single-crystal films of beryllium on alpha-AI2O3 (sapphire), silicon, and germanium using molecular beam epitaxy (MBE). This is a major development since beryllium is an excellent spacer for the difficult but desirable water window wavelengths (24 A < lambda < 44 A). To our knowledge, this is the first time beryllium has been grown epitaxially on any substrate. Our best quality beryllium films were grown on silicon. The ability to grow a single crystal layer of beryllium is a promising first step toward a beryllium-based single-crystal mirror. In the area of new material pairs. we began by using theoretical reflectivity calculations to assemble a list of promising new material pairs. We then prioritized this list by using what was already known about the materials, such as phase diagrams and diffusion studies. These materials pairs then were studied by sputtering and/or MBE.

Limitations: APPROVED FOR PUBLIC RELEASE
Description: Final rept. 1 Jan 90-28 Feb 93
Pages: 9
Report Date: 29 APR 93
Contract Number: AFOSR-90-0140
Report Number: A941762
Keywords relating to this report:
*BERYLLIUM
*EPITAXIAL GROWTH
*OPTICS
*SINGLE CRYSTALS
*X RAYS
ALUMINUM OXIDES
BORON
CARBIDES
COMPOSITE MATERIALS
DIFFUSION
FILMS
GERMANIUM
INTERFACES
LAYERS
MIRRORS
MOLECULAR BEAMS
MOLYBDENUM
OPTICAL PROPERTIES
PALLADIUM
PHASE DIAGRAMS
REFLECTIVITY
SAPPHIRE
SILICON
SPACERS
SUBSTRATES
TITANIUM
TUNGSTEN
X RAY DIFFRACTION
X RAY SCATTERING
YTTRIUM
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