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ChemistryIndustrial Chemistry and Chemical Processing

Evolution of the gamma/gamma' Interface Width in a Commercial Nickel Base Superalloy Studied by 3D Atom Probe (Preprint)

Authors: J Tiley; J Y Hwang; R Banerjee; R Srinivasan; H L Fraser; S Nag; A R Singh; NORTH TEXAS STATE UNIV DENTON
Abstract:
The compositional width of the gamma/gamma-prime interface for primary and secondary gamma-prime precipitates in the commercial nickel base superalloy, Rene 88 DT, has been characterized at sub-nanometer resolution using local electrode atom probe (LEAP) tomography. On formation during continuous cooling, the primary gamma-prime precipitates exhibit a very sharp interface while the secondary gamma-prime precipitates exhibit a substantially more diffuse interface. Interestingly, on subsequent isothermal aging at 760 degrees C, the interface width increases for the primary gamma-prime precipitates while it decreases for the secondary gamma-prime precipitates, reaching a near equilibrium composition width for both types of interfaces after aging for 200 hours. These results imply the gamma/gamma-prime interface width is strongly dependent on temperature in these alloys.

Limitations: APPROVED FOR PUBLIC RELEASE
Description: Journal article preprint
Pages: 15
Report Date: Mar-2009
Contract Number: FA8650-08-C-5226 FA865008C5226
Report Number: A096205
Keywords relating to this report:
*NANOSTRUCTURES
*NICKEL ALLOYS
*Probes
*SUPERALLOYS
AGING_MATERIALS_
COMPOSITION_PROPERTY_
COOLING
DIFFUSION
ELECTRODES
INTERFACES
ISOTHERMS
THREE DIMENSIONAL
TOMOGRAPHY
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